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Research Paper | Chemical Sciences | Iraq | Volume 6 Issue 11, November 2017
Synthesis of New Poly (Subs- Vinyl Malonate Amine) from Malonyl Chloride
Entesar O. Al-Tamimi [2] | Noor Ahmed Ali [3]
Abstract: New polymers were prepared by malonyl chloride. malonyl choride was prepared from malonic acid, these polymers were prepared by several steps. The first step was included reaction of poly vinyl alcohol with malonyl chloride to produce poly vinyl malonate (1). Second step was reacted of poly sodium vinyl malonate with different alkyl halide (3-6). Bromine was added to produce polymers in third step (7-10). The last step was added different amines (primary and secondary amines) to prepared poly [ (2-alkyl amino-2-alkyl) vinyl malonate] [ (11-18), (19-30)]. All the prepared polymers were characterized by FT-IR, and some of them 1H-NMR, and measured some of different physical properties as, solubility and softening point.
Keywords: malonic acid, polyvinyl alcohol, polyester, polyamine
Edition: Volume 6 Issue 11, November 2017,
Pages: 429 - 435
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