Synthesis and Characterization of New Complexes of 2- (2-Hydroxy Phenyl)-2-N-Amino (4-Chloro-Benzothiazol-2-Yl) Acetonitrile Ligand with Some Divalent Transition Metal Ions
International Journal of Science and Research (IJSR)

International Journal of Science and Research (IJSR)
Call for Papers | Fully Refereed | Open Access | Double Blind Peer Reviewed

ISSN: 2319-7064


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Research Paper | Chemistry | Iraq | Volume 3 Issue 11, November 2014 | Popularity: 6.2 / 10


     

Synthesis and Characterization of New Complexes of 2- (2-Hydroxy Phenyl)-2-N-Amino (4-Chloro-Benzothiazol-2-Yl) Acetonitrile Ligand with Some Divalent Transition Metal Ions

Mohammed H. A. Al-Amery


Abstract: A series of metal complexes of some divalent transition metal ions [MnII, CoII, NiII, CuII, ZnII, CdII, HgII] having the general composition [ML2Cl2]. nH2O with bidentate 2- (2-hydroxy phenyl) -2-N-amino (4-chloro- benzothiazol-2-yl) acetonitrile ligand which was prepared from 2-hydroxy-benzaldehyde and 5-chlorobenzo [d]thiazol-2-amine in the presence of KCN and acidic medium have been prepared and characterized by elemental chemical analysis (CHNS), molar conductance, magnetic susceptibility measurements, 1H-NMR spectra, FTIR electronic spectral studies and Atomic Absorption Technique. The FTIR spectral data suggest the involvement of amino and acetonitrile nitrogen in coordination to central metal ion. On the basis of spectral studies, an octahedral geometry has been assigned for the divalent transition metal complexes.


Keywords: 2- 2-hydroxy phenyl -2-N-amino 4-chloro-benzothiazol-2-yl acetonitrile, bidentate, divalent, transition metals


Edition: Volume 3 Issue 11, November 2014


Pages: 3059 - 3064



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Mohammed H. A. Al-Amery, "Synthesis and Characterization of New Complexes of 2- (2-Hydroxy Phenyl)-2-N-Amino (4-Chloro-Benzothiazol-2-Yl) Acetonitrile Ligand with Some Divalent Transition Metal Ions", International Journal of Science and Research (IJSR), Volume 3 Issue 11, November 2014, pp. 3059-3064, https://www.ijsr.net/getabstract.php?paperid=SUB1461, DOI: https://www.doi.org/10.21275/SUB1461

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