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Research Paper | Chemistry | Iraq | Volume 6 Issue 8, August 2017
Synthesis of New Poly (Subs- Vinyl Malonate Amide) from Malonic Acid
Entessar O. Al-Tamimi | Noor Ahmed Ali [3]
Abstract: New polymers were prepared by modification of malonic acid, these polymers were prepared by several steps. The first step was included reaction of poly vinyl alcohol with malonyl chloride to produce poly vinyl malonate. Second step was included reaction of poly sodium vinyl malonate with different alkyl halide. Bromine in was added to produce polymers in third step, and then added ammonia to prepared polymers to form poly amino alkyl vinyl malonate. The last step was reacted poly amino malonate with acid chloride [ (acetyl, benzoyl) chloride] in DMF. All the prepared polymers were characterized by FT-IR, H-NMR, and measured some of different physical properties as, solubility and softening point.
Keywords: malonic acid, polyvinyl alcohol, polyester-amide
Edition: Volume 6 Issue 8, August 2017,
Pages: 1883 - 1888