Esterification Reaction for Novel Synthesis Castor-Based Polyester and Formulation as Base Oil in Synthetic Drilling Fluid
International Journal of Science and Research (IJSR)

International Journal of Science and Research (IJSR)
www.ijsr.net | Open Access | Fully Refereed | Peer Reviewed International Journal

ISSN: 2319-7064



Downloads: 108 | Weekly Hits: ⮙1 | Monthly Hits: ⮙9

Research Paper | Chemistry | Egypt | Volume 3 Issue 12, December 2014

Esterification Reaction for Novel Synthesis Castor-Based Polyester and Formulation as Base Oil in Synthetic Drilling Fluid

S. Ibrahim

Ricinoleic acid [hydroxyl fatty acid] is the meager constituent fatty acid in castor oil (85 95 %). Castor oil is inedible oil which is one of the crops available, reachable oil in Egypt. Novel polyesters produced form esterification of different ratios of hydroxyl fatty acid (35, 55, and 75 %) with glycerol and phthalic anhydride, at temperatures between 120 and 240C. Three different novel polyesters were collected and designated as HD35, HD55 and HD75 respectively. The average degree of polymerization is monitoring by determining the acid number of the aliquot of the reaction mixture and by measuring the volume of water evolved. The chemical structure of the new prepared polyesters were elucidated using Faurier transform infrared (FTIR) spectrophotometer, and the molecular weight determinations were conducted by Mass spectrophotometer. The average molecular weight of the novel polyesters compound ranged from 980 to 1500. The biodegradability of the new prepared polyesters gives us good indications the ability to be environmentally friendly. The new prepared polyesters were formulated and evaluated as a synthetic based mud (esterbased mud) for oilwell drilling fluids. The evaluation includes study of the rheological properties, filtration and thermal stability of both reference commercial esterbased mud and ester basedmuds formulated with the new prepared polyesters according to AIP specifications.

Keywords: Inedible Oils, Castor Oil, EsterBased Mud, Biodegradation

Edition: Volume 3 Issue 12, December 2014

Pages: 1969 - 1975

Share this Article

How to Cite this Article?

S. Ibrahim, "Esterification Reaction for Novel Synthesis Castor-Based Polyester and Formulation as Base Oil in Synthetic Drilling Fluid", International Journal of Science and Research (IJSR), https://www.ijsr.net/search_index_results_paperid.php?id=SUB14855, Volume 3 Issue 12, December 2014, 1969 - 1975

Enter Your Email Address




Similar Articles with Keyword 'Castor Oil'

Downloads: 127

Review Papers, Chemistry, India, Volume 5 Issue 2, February 2016

Pages: 1786 - 1791

A Review on Biodegradable Polymeric Materials Derived from Vegetable Oils for Diverse Applications

Abhishek Chowdhury, Prashant Anthony

Share this Article

Downloads: 134

Research Paper, Chemistry, India, Volume 5 Issue 9, September 2016

Pages: 159 - 161

Modification of Asphalt using Castor Oil Based Polyurethane

Mandar Karve, Nirmal K. Patel, Subhash Polara

Share this Article

Similar Articles with Keyword 'Oils'

Downloads: 127

Research Paper, Chemistry, Nigeria, Volume 2 Issue 4, April 2013

Pages: 463 - 467

Heavy Metal Analysis of Blends of Methyl Esters Obtained from Four Virgin Tropical Seed Oils

O. G. Igbum, K. Asemave, C. A Nwadinigwe, N. Y. Akaasah

Share this Article

Downloads: 13

Comparative Studies, Chemistry, India, Volume 10 Issue 4, April 2021

Pages: 831 - 840

Comparative Studies on Soil Quality Evaluation (For Heavy Metals) in Coastal Region of PSR Nellore Dist, Andhra Pradesh, India

C. Masthan, P. Muni Nagendra Prasad, O. Audi Seshaiah, Y. V. Rami Reddy

Share this Article

Similar Articles with Keyword 'Castor'

Downloads: 127

Review Papers, Chemistry, India, Volume 5 Issue 2, February 2016

Pages: 1786 - 1791

A Review on Biodegradable Polymeric Materials Derived from Vegetable Oils for Diverse Applications

Abhishek Chowdhury, Prashant Anthony

Share this Article

Downloads: 134

Research Paper, Chemistry, India, Volume 5 Issue 9, September 2016

Pages: 159 - 161

Modification of Asphalt using Castor Oil Based Polyurethane

Mandar Karve, Nirmal K. Patel, Subhash Polara

Share this Article

Similar Articles with Keyword 'Oil'

Downloads: 127

Research Paper, Chemistry, Nigeria, Volume 2 Issue 4, April 2013

Pages: 463 - 467

Heavy Metal Analysis of Blends of Methyl Esters Obtained from Four Virgin Tropical Seed Oils

O. G. Igbum, K. Asemave, C. A Nwadinigwe, N. Y. Akaasah

Share this Article

Downloads: 13

Comparative Studies, Chemistry, India, Volume 10 Issue 4, April 2021

Pages: 831 - 840

Comparative Studies on Soil Quality Evaluation (For Heavy Metals) in Coastal Region of PSR Nellore Dist, Andhra Pradesh, India

C. Masthan, P. Muni Nagendra Prasad, O. Audi Seshaiah, Y. V. Rami Reddy

Share this Article

Similar Articles with Keyword 'Mud'

Downloads: 119

Research Paper, Chemistry, India, Volume 7 Issue 7, July 2018

Pages: 1401 - 1406

Earthworm Excreta: A Helping Hand for the Production of Fuel Ethanol

Prakhar Bhatnagar, Mohammad Azhar

Share this Article

Downloads: 148 | Weekly Hits: ⮙1 | Monthly Hits: ⮙1

Research Paper, Chemistry, India, Volume 7 Issue 1, January 2018

Pages: 1278 - 1281

Treatments of Water Pollutants of Agyara Dam (Hans Sarowar Dam), at Matsya Industrial Area, Alwar by Moringa Oleifera Seeds (Adsorption Medias)

Rajendra Singh Meena, Dr. Ritu Mathur, Dr. M. P. S. Chandrawat, Dr. V. P. Bairwa

Share this Article



Top