International Journal of Science and Research (IJSR)

International Journal of Science and Research (IJSR)
Open Access | Fully Refereed | Peer Reviewed

ISSN: 2319-7064


Downloads: 152

Research Paper | Chemical Sciences | Tunisia | Volume 7 Issue 7, July 2018


Optimization of Conditions for the synthesis of new Triphenylphosphonium-Substituted phthalocyanine from Tetrabrominated Phthalocyanine using Experimental Design Method

Mohamed Tarhouni, Fabienne Dumoulin, Bassem Jamoussi


Abstract: An experimental design has been drawn up to optimize the experimental conditions of the synthesis of new Triphenylphosphonium-substituted phthalocyanine from tetrabrominated phthalocyanine. Response surface methodology (RSM) was applied to study the influence of molar ratio of tetrabrominated phthalocyanine to triphenylphosphine, reaction time and the reaction temperature. Quadratic model was developed for yield of Triphenylphosphonium-substituted phthalocyanine using Design-Expert software NEMRODW. The model was used to calculate the optimum operating conditions for synthesis of Triphenylphosphonium-substituted phthalocyanine. The optimum conditions were obtained as follows n (tetrabrominated phthalocyanine TTBPc) n (triphenylphosphinePPh3) = 120, reaction time 12 h and reaction temperature 120C. Under these conditions, the yield of Triphenylphosphonium-substituted phthalocyanine reached 70 %.


Keywords: Triphenylphosphonium-substituted phthalocyanine, tetrabrominated phthalocyanine, Response surface methodology


Edition: Volume 7 Issue 7, July 2018,


Pages: 65 - 70


How to Cite this Article?

Mohamed Tarhouni, Fabienne Dumoulin, Bassem Jamoussi, "Optimization of Conditions for the synthesis of new Triphenylphosphonium-Substituted phthalocyanine from Tetrabrominated Phthalocyanine using Experimental Design Method", International Journal of Science and Research (IJSR), https://www.ijsr.net/get_abstract.php?paper_id=ART20183736, Volume 7 Issue 7, July 2018, 65 - 70

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